Continuously Stirred Tank Reactor#

In this example we will illustrate how Cantera can be used to simulate a continuously stirred tank reactor (CSTR), also interchangeably referred to as a perfectly stirred reactor (PSR), a well stirred reactor (WSR), a jet stirred reactor (JSR), or a Longwell reactor (and there may well be more “aliases”).

Requires: cantera >= 3.0, matplotlib >= 2.0, pandas

Tags: Python combustion reactor network well-stirred reactor

Simulation of a CSTR/PSR/WSR#

A diagram of a CSTR is shown below:

A continuously stirred tank reactor with inflow and outflow

As the figure illustrates, this is an open system (unlike a batch reactor, which is isolated). P, V and T are the reactor’s pressure, volume and temperature respectively. The mass flow rate at which reactants come in is the same as that of the products which exit, and on average this mass stays in the reactor for a characteristic time \(\tau\), called the residence time. This is a key quantity in sizing the reactor and is defined as follows:

\[\tau = \frac{m}{\dot{m}}\]

where \(m\) is the mass of the gas.

Import modules and set plotting defaults#

import time
from io import StringIO
import matplotlib.pyplot as plt
import pandas as pd
import cantera as ct

print(f"Running Cantera version: {ct.__version__}")
Running Cantera version: 3.1.0

Define the gas#

In this example, we will work with n-C₇H₁₆/O₂/He mixtures, for which experimental data can be found in the paper by Zhang et al. [1] We will use the same mechanism reported in the paper. It consists of 1268 species and 5336 reactions.

gas = ct.Solution("example_data/n-hexane-NUIG-2015.yaml")

Define initial conditions#

Inlet conditions for the gas and reactor parameters#

reactor_temperature = 925  # Kelvin
reactor_pressure = 1.046138 * ct.one_atm  # in atm. This equals 1.06 bars
inlet_concentrations = {"NC7H16": 0.005, "O2": 0.0275, "HE": 0.9675}
gas.TPX = reactor_temperature, reactor_pressure, inlet_concentrations

residence_time = 2  # s
reactor_volume = 30.5 * (1e-2) ** 3  # m3

Simulation parameters#

# Simulation termination criterion
max_simulation_time = 50  # seconds

Reactor arrangement#

We showed a cartoon of the reactor in the first figure in this notebook, but to actually simulate that, we need a few peripherals. A mass-flow controller upstream of the stirred reactor will allow us to flow gases in, and in-turn, a “reservoir” which simulates a gas tank is required to supply gases to the mass flow controller. Downstream of the reactor, we install a pressure regulator which allows the reactor pressure to stay within. Downstream of the regulator we will need another reservoir which acts like a “sink” or capture tank to capture all exhaust gases (even our simulations are environmentally friendly!). This arrangement is illustrated below:

A complete reactor network representing a continuously stirred tank reactor

Initialize the stirred reactor and connect all peripherals#

fuel_air_mixture_tank = ct.Reservoir(gas)
exhaust = ct.Reservoir(gas)

stirred_reactor = ct.IdealGasMoleReactor(gas, energy="off", volume=reactor_volume)

mass_flow_controller = ct.MassFlowController(
    upstream=fuel_air_mixture_tank,
    downstream=stirred_reactor,
    mdot=stirred_reactor.mass / residence_time,
)

pressure_regulator = ct.PressureController(
    upstream=stirred_reactor,
    downstream=exhaust,
    primary=mass_flow_controller,
    K=1e-3,
)

reactor_network = ct.ReactorNet([stirred_reactor])

# Create a SolutionArray to store the data
time_history = ct.SolutionArray(gas, extra=["t"])

# Set the maximum simulation time
max_simulation_time = 50  # seconds

# Start the stopwatch
tic = time.time()

# Set simulation start time to zero
t = 0
counter = 1
while t < max_simulation_time:
    t = reactor_network.step()

    # We will store only every 10th value. Remember, we have 1200+ species, so there
    # will be 1200+ columns for us to work with
    if counter % 10 == 0:
        # Extract the state of the reactor
        time_history.append(stirred_reactor.thermo.state, t=t)

    counter += 1

# Stop the stopwatch
toc = time.time()

print(f"Simulation Took {toc-tic:3.2f}s to compute, with {counter} steps")
Simulation Took 6.09s to compute, with 355 steps

Plot the results#

As a test, we plot the mole fraction of CO and see if the simulation has converged. If not, go back and adjust max. number of steps and/or simulation time.

plt.figure()
plt.semilogx(time_history.t, time_history("CO").X, "-o")
plt.xlabel("Time (s)")
plt.ylabel("Mole Fraction : $X_{CO}$")
continuous reactor

Illustration : Modeling experimental data#

Let us see if the reactor can reproduce actual experimental measurements.

We first load the data. This is also supplied in the paper by Zhang et al. [1] as an excel sheet

experimental_data_csv = """
T,NC7H16,O2,CO,CO2
500,5.07E-03,2.93E-02,0.00E+00,0.00E+00
525,4.92E-03,2.86E-02,0.00E+00,0.00E+00
550,4.66E-03,2.85E-02,0.00E+00,0.00E+00
575,4.16E-03,2.63E-02,2.43E-04,1.01E-04
600,3.55E-03,2.33E-02,9.68E-04,2.51E-04
625,3.36E-03,2.31E-02,1.42E-03,2.67E-04
650,3.67E-03,2.45E-02,9.16E-04,1.46E-04
675,4.38E-03,2.77E-02,2.25E-04,0.00E+00
700,4.79E-03,2.87E-02,0.00E+00,0.00E+00
725,4.89E-03,2.93E-02,0.00E+00,0.00E+00
750,4.91E-03,2.84E-02,0.00E+00,0.00E+00
775,4.93E-03,2.80E-02,0.00E+00,0.00E+00
800,4.78E-03,2.82E-02,0.00E+00,0.00E+00
825,4.41E-03,2.80E-02,1.49E-05,0.00E+00
850,3.68E-03,2.80E-02,4.18E-04,1.66E-04
875,2.13E-03,2.45E-02,1.65E-03,2.22E-04
900,1.03E-03,2.05E-02,5.51E-03,3.69E-04
925,5.82E-04,1.79E-02,8.59E-03,6.78E-04
950,3.88E-04,1.47E-02,1.05E-02,1.07E-03
975,2.35E-04,1.28E-02,1.19E-02,1.36E-03
1000,1.14E-04,1.16E-02,1.34E-02,1.82E-03
1025,4.83E-05,9.88E-03,1.52E-02,2.41E-03
1050,1.64E-05,8.16E-03,1.83E-02,2.97E-03
1075,1.22E-06,5.48E-03,1.95E-02,3.67E-03
1100,0.00E+00,3.24E-03,2.14E-02,4.38E-03
"""

experimental_data = pd.read_csv(StringIO(experimental_data_csv))
experimental_data.head()
T NC7H16 O2 CO CO2
0 500 0.00507 0.0293 0.000000 0.000000
1 525 0.00492 0.0286 0.000000 0.000000
2 550 0.00466 0.0285 0.000000 0.000000
3 575 0.00416 0.0263 0.000243 0.000101
4 600 0.00355 0.0233 0.000968 0.000251


# Define all the temperatures at which we will run simulations. These should overlap
# with the values reported in the paper as much as possible
T = [650, 700, 750, 775, 825, 850, 875, 925, 950, 1075, 1100]

# Create a SolutionArray to store values for the above points
temp_dependence = ct.SolutionArray(gas)

Now we simply run the reactor code we used above for each temperature

Simulation at T=650 K took 8.38 s to compute with 1196 steps
Simulation at T=700 K took 6.67 s to compute with 1039 steps
Simulation at T=750 K took 4.16 s to compute with 718 steps
Simulation at T=775 K took 3.75 s to compute with 585 steps
Simulation at T=825 K took 5.04 s to compute with 829 steps
Simulation at T=850 K took 5.55 s to compute with 856 steps
Simulation at T=875 K took 5.01 s to compute with 817 steps
Simulation at T=925 K took 5.32 s to compute with 894 steps
Simulation at T=950 K took 4.67 s to compute with 742 steps
Simulation at T=1075 K took 5.60 s to compute with 965 steps
Simulation at T=1100 K took 4.39 s to compute with 711 steps

Compare the model results with experimental data#

plt.figure()
plt.plot(
    temp_dependence.T, temp_dependence("NC7H16").X, color="C0", label="$nC_{7}H_{16}$"
)
plt.plot(temp_dependence.T, temp_dependence("CO").X, color="C1", label="CO")
plt.plot(temp_dependence.T, temp_dependence("O2").X, color="C2", label="O$_{2}$")

plt.plot(
    experimental_data["T"],
    experimental_data["NC7H16"],
    color="C0",
    marker="o",
    label="$nC_{7}H_{16}$ (exp)",
)
plt.plot(
    experimental_data["T"],
    experimental_data["CO"],
    color="C1",
    marker="^",
    linestyle="none",
    label="CO (exp)",
)
plt.plot(
    experimental_data["T"],
    experimental_data["O2"],
    color="C2",
    marker="s",
    linestyle="none",
    label="O$_2$ (exp)",
)

plt.xlabel("Temperature (K)")
plt.ylabel(r"Mole Fractions")

plt.xlim([650, 1100])
plt.legend(loc=1)
continuous reactor

References#

Total running time of the script: (1 minutes 5.217 seconds)

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